By Nicholas P. Vakar

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With this process, there is no removal of free fatty acids. The free fatty acid removal is accomplished later in the deodorization process. Compared to caustic refining, the merits of this process include improving yield performance and eliminating the soapstock disposal problems. E. Staley Manufacturing Co. used acid refining (acetic anhydride) for over 30 years. In recent years, AGP has developed, used, and promoted acid refining (citric acid). Several edible oil refiners throughout the world have used phosphoric acid in acid refining.

If the analytical results of the second sample fail, the shipment should be rejected. Any further sampling and analysis of the oil would be counterproductive. When it is found that the critical analytical results meet the purchase specifications, authori­zation can be given to unload the oil. Tank cars should not be unloaded until all the analyses are com­pleted. J. Smallwood value, filter test, flavor, and refractive index) com­pare favorably with the supplier’s certificate of analysis and meet product specifications.

Nitrogen is preferable, but air can be used if nitrogen is not available. 15. Disconnect the unloading hose and cap the open end. 16. Secure the unloading hose to prevent damage in the traffic area. 17. Measure the quantity of oil in the storage tank and compare the volume gain to the quantity of oil contained in the transport vessel. 18. Obtain and analyze a representative sample of oil from the storage tank. Compare the results from the tank sample to the results from the pre-unloading sample.

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